ASTM D3616-1995(2004)e1 测定生橡胶的凝胶、膨胀指数及衡释溶液粘度的标准试验方法

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【英文标准名称】:StandardTestMethodforRubber,Raw-DeterminationofGel,SwellingIndex,andDiluteSolutionViscosity
【原文标准名称】:测定生橡胶的凝胶、膨胀指数及衡释溶液粘度的标准试验方法
【标准号】:ASTMD3616-1995(2004)e1
【标准状态】:现行
【国别】:
【发布日期】:1995
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D11.11
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:合成橡胶;试验;炭黑;测定;凝胶;粘度;橡胶;膨胀指数;天然橡胶
【英文主题词】:dilutesolutionviscosity;DSV;gel;rawrubber;swellingindex
【摘要】:Thesetestsareparticularlyusefulforqualitycontrolintheproductionofsyntheticrubbers.Percentgelisameasureoftheamountofinsolublerubberpresentinthechosensolvent.Gelmaybeintroducedintentionallyinsomerubbers.Variationsfromanormallevelindicatechangesinthepolymerizationsystem.Swellingindexisameasureofthetypeofgel.Gelwithalow-swellingindexisreferredtoasx201C;hardgelx201D;andusuallyindicatesthepresenceofmaterialthatdoesnotbreakdownreadilybymilling.Ahigh-swellingindexnormallyindicatesthepresenceofax201C;loosegelx201D;thatmaybebrokendowneasilybymilling.Inlow-gelorgel-freerubbers,theDSVcorrelatesdirectlywiththemolecularweight.Sincetheviscosityismeasuredonlyonthesolubleportionoftherubber,theuseofDSVtopredictmolecularweightinrubbershavinghighgelvaluesismeaningless.1.1Thistestmethodcoversthedeterminationofthedilutesolutionviscosity(DSV),thegelcharacteristics,andtheswellingindexofrawnon-oil-extendedandnon-pigmentedSBRandNBR.1.2ThistestmethodmaybeusedtodeterminetheDSVandgelcharacteristicsofrubbersotherthanSBRandNBR,however,solventsotherthan2-butanoneandtoluenemayberequired.1.3Thistestmethodisnotintendedforthemeasurementofmicro-gel.Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.
【中国标准分类号】:G34
【国际标准分类号】:83_040_10
【页数】:5P.;A4
【正文语种】: