ISO 13885-1-2008 涂料和清漆用粘合剂.凝胶渗透色谱法(GPC).第1部分:用四氢呋喃(THF)作洗提液
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【英文标准名称】:Bindersforpaintsandvarnishes-Gelpermeationchromatography(GPC)-Part1:Tetrahydrofuran(THF)aseluent
【原文标准名称】:涂料和清漆用粘合剂.凝胶渗透色谱法(GPC).第1部分:用四氢呋喃(THF)作洗提液
【标准号】:ISO13885-1-2008
【标准状态】:现行
【国别】:国际
【发布日期】:2008-08
【实施或试行日期】:
【发布单位】:国际标准化组织(IX-ISO)
【起草单位】:ISO/TC35
【标准类型】:()
【标准水平】:()
【中文主题词】:器具;粘合剂;校正;化学分析和测试;色谱;色谱法;涂层材料;覆层;定义;含量测定;凝胶渗透色谱法;凝胶;GPC;高效液相色谱法;高效液相色谱分析法;调查;液相色谱法;测量;摩尔质量;涂料;渗透;塑料;高聚物;试样制备;试验设备;测试;四氢呋喃;清漆
【英文主题词】:Apparatus;Bindingagents;Calibration;Chemicalanalysisandtesting;Chromatograms;Chromatography;Coatingmaterials;Coatings;Definitions;Determinationofcontent;Gelpermeationchromatography;Gels;GPC;Highperformanceliquidchromatography;HPLC;Investigations;Liquidchromatography;Measurement;Molarmass;Paints;Permeation;Plastics;Polymers;Specimenpreparation;Testequipment;Testing;Tetrahydrofuran;Varnishes
【摘要】:ThispartofISO13885describesthedeterminationofthemolar-massdistribution,number-averagemolarmassMnandmass-averagemolarmassMwofpolymersthataresolubleinTHF(tetrahydrofuran)bygelpermeationchromatography(GPC)I).Itispossiblethat,inspiteofthegoodrepeatabilityobtainedwiththismethod,itcannotbeusedwithcertainpolymertypesbecauseofspecificinteractions,suchasadsorptionwithinthesample/eluentJcolumnsystem.Themethodisnotanabsoluteoneandrequirescalibrationwithcommerciallyavailableunbranched-polystyrenestandardsthathavebeencharacterizedbyabsolutemethods.Theresultsforsamplesofpolymersotherthanpolystyrenearethereforeonlycomparablewithingroupsofsamplesofthesametype.TheconditionsspecifiedinthispartofISO13885arenotsuitablefortheGPCanalysisofpolymersampleswith.~/wvaluesgreaterthan106(seeAnnexC).Nocorrectionmethods,e.g.fortheeliminationofpeakbroadening,areincludedinthispartofISO13885.Ifabsolutemolar-massvaluesarerequired,anabsolutemethod,e.g.membraneosmometryfor.UnorlightscatteringforMw,mustbeused.
【中国标准分类号】:G52
【国际标准分类号】:87_060_20
【页数】:22P;A4
【正文语种】:英语
【原文标准名称】:涂料和清漆用粘合剂.凝胶渗透色谱法(GPC).第1部分:用四氢呋喃(THF)作洗提液
【标准号】:ISO13885-1-2008
【标准状态】:现行
【国别】:国际
【发布日期】:2008-08
【实施或试行日期】:
【发布单位】:国际标准化组织(IX-ISO)
【起草单位】:ISO/TC35
【标准类型】:()
【标准水平】:()
【中文主题词】:器具;粘合剂;校正;化学分析和测试;色谱;色谱法;涂层材料;覆层;定义;含量测定;凝胶渗透色谱法;凝胶;GPC;高效液相色谱法;高效液相色谱分析法;调查;液相色谱法;测量;摩尔质量;涂料;渗透;塑料;高聚物;试样制备;试验设备;测试;四氢呋喃;清漆
【英文主题词】:Apparatus;Bindingagents;Calibration;Chemicalanalysisandtesting;Chromatograms;Chromatography;Coatingmaterials;Coatings;Definitions;Determinationofcontent;Gelpermeationchromatography;Gels;GPC;Highperformanceliquidchromatography;HPLC;Investigations;Liquidchromatography;Measurement;Molarmass;Paints;Permeation;Plastics;Polymers;Specimenpreparation;Testequipment;Testing;Tetrahydrofuran;Varnishes
【摘要】:ThispartofISO13885describesthedeterminationofthemolar-massdistribution,number-averagemolarmassMnandmass-averagemolarmassMwofpolymersthataresolubleinTHF(tetrahydrofuran)bygelpermeationchromatography(GPC)I).Itispossiblethat,inspiteofthegoodrepeatabilityobtainedwiththismethod,itcannotbeusedwithcertainpolymertypesbecauseofspecificinteractions,suchasadsorptionwithinthesample/eluentJcolumnsystem.Themethodisnotanabsoluteoneandrequirescalibrationwithcommerciallyavailableunbranched-polystyrenestandardsthathavebeencharacterizedbyabsolutemethods.Theresultsforsamplesofpolymersotherthanpolystyrenearethereforeonlycomparablewithingroupsofsamplesofthesametype.TheconditionsspecifiedinthispartofISO13885arenotsuitablefortheGPCanalysisofpolymersampleswith.~/wvaluesgreaterthan106(seeAnnexC).Nocorrectionmethods,e.g.fortheeliminationofpeakbroadening,areincludedinthispartofISO13885.Ifabsolutemolar-massvaluesarerequired,anabsolutemethod,e.g.membraneosmometryfor.UnorlightscatteringforMw,mustbeused.
【中国标准分类号】:G52
【国际标准分类号】:87_060_20
【页数】:22P;A4
【正文语种】:英语
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